Schöniger oxidation
Encyclopedia
In chemistry
, the Schöniger oxidation (also known as the Schöniger flask test or the oxygen flask method) is a method of elemental analysis
developed by Wolfgang Schöniger.
The test is conducted in an Erlenmeyer flask
, or in a separatory funnel
. It involves the combustion of a sample in pure oxygen, followed by the absorption of the combustion products by a solution of sodium hydroxide.
It allows quantitative determination of elemental chlorine
, nitrogen
and sulfur
in a sample.
Chemistry
Chemistry is the science of matter, especially its chemical reactions, but also its composition, structure and properties. Chemistry is concerned with atoms and their interactions with other atoms, and particularly with the properties of chemical bonds....
, the Schöniger oxidation (also known as the Schöniger flask test or the oxygen flask method) is a method of elemental analysis
Elemental analysis
Percent Composition is a process where a sample of some material is analyzed for its elemental and sometimes isotopic composition. Elemental analysis can be qualitative , and it can be quantitative...
developed by Wolfgang Schöniger.
The test is conducted in an Erlenmeyer flask
Erlenmeyer flask
An Erlenmeyer flask, also known as a conical flask, is a widely used type of laboratory flask which features a flat bottom, a conical body, and a cylindrical neck. It is named after the German chemist Emil Erlenmeyer, who created it in 1861...
, or in a separatory funnel
Separatory funnel
A separatory funnel, also known as separation funnel, separating funnel, or colloquially sep funnel, is a piece of laboratory glassware used in liquid-liquid extractions to separate the components of a mixture between two immiscible solvent phases of different densities Typically, one of the...
. It involves the combustion of a sample in pure oxygen, followed by the absorption of the combustion products by a solution of sodium hydroxide.
It allows quantitative determination of elemental chlorine
Chlorine
Chlorine is the chemical element with atomic number 17 and symbol Cl. It is the second lightest halogen, found in the periodic table in group 17. The element forms diatomic molecules under standard conditions, called dichlorine...
, nitrogen
Nitrogen
Nitrogen is a chemical element that has the symbol N, atomic number of 7 and atomic mass 14.00674 u. Elemental nitrogen is a colorless, odorless, tasteless, and mostly inert diatomic gas at standard conditions, constituting 78.08% by volume of Earth's atmosphere...
and sulfur
Sulfur
Sulfur or sulphur is the chemical element with atomic number 16. In the periodic table it is represented by the symbol S. It is an abundant, multivalent non-metal. Under normal conditions, sulfur atoms form cyclic octatomic molecules with chemical formula S8. Elemental sulfur is a bright yellow...
in a sample.