Annular dark-field imaging
Encyclopedia
Annular dark-field imaging is a method of mapping samples in a scanning transmission electron microscope (STEM). These images are formed by collecting scattered electrons with an annular dark-field detector.
In traditional dark-field imaging, an objective aperture is placed in the diffraction plane so as to only collect electrons scattering through that aperture, avoiding the main beam.
An annular dark field detector collects electrons from an annulus around the beam, sampling far more scattered electrons than can pass through an objective aperture. This gives an advantage in terms of signal collection efficiency and allows the main beam to pass to an EELS
detector, allowing both types of measurement to be performed simultaneously.
An annular dark field image formed only by very high angle, incoherently scattered electrons — as opposed to Bragg scattered electrons — is highly sensitive to variations in the atomic number of atoms in the sample (Z-contrast images). This technique is also known as high-angle annular dark-field imaging (HAADF).
In traditional dark-field imaging, an objective aperture is placed in the diffraction plane so as to only collect electrons scattering through that aperture, avoiding the main beam.
An annular dark field detector collects electrons from an annulus around the beam, sampling far more scattered electrons than can pass through an objective aperture. This gives an advantage in terms of signal collection efficiency and allows the main beam to pass to an EELS
Electron energy loss spectroscopy
In electron energy loss spectroscopy a material is exposed to a beam of electrons with a known, narrow range of kinetic energies. Some of the electrons will undergo inelastic scattering, which means that they lose energy and have their paths slightly and randomly deflected...
detector, allowing both types of measurement to be performed simultaneously.
An annular dark field image formed only by very high angle, incoherently scattered electrons — as opposed to Bragg scattered electrons — is highly sensitive to variations in the atomic number of atoms in the sample (Z-contrast images). This technique is also known as high-angle annular dark-field imaging (HAADF).