Sand bath
Encyclopedia
A sand bath is a common piece of laboratory equipment made from a container filled with heated sand
. It is used to provide even heating for another container, most often during a chemical reaction
.
A sand bath is most commonly used in conjunction with a hot plate
or heating mantle
. A beaker
is filled with sand or metal pellets (called shot
) and is placed on the plate or mantle. The reaction vessel is then partially covered by sand or pellets. The sand or shot then conducts the heat from the plate to all sides of the reaction vessel.
This technique allows a reaction vessel to be heated throughout with minimal stirring, as opposed to heating the bottom of the vessel and waiting for convection
to heat the remainder, cutting down on both the duration of the reaction and the possibility of side reactions that may occur at higher temperatures.
A variation on this theme is the water bath
in which the sand is replaced with water. It can be used to keep a reaction vessel at the temperature of boiling water until all water is evaporated (see Standard enthalpy change of vaporization
).
Sand baths are one of the oldest known pieces of laboratory equipment, having been used by the alchemists
. In Arabic alchemy, a sand bath was known as a qadr. In Latin
alchemy, a sand bath was called balneum siccum, balneum cineritium, or balneum arenosum.
Sand
Sand is a naturally occurring granular material composed of finely divided rock and mineral particles.The composition of sand is highly variable, depending on the local rock sources and conditions, but the most common constituent of sand in inland continental settings and non-tropical coastal...
. It is used to provide even heating for another container, most often during a chemical reaction
Chemical reaction
A chemical reaction is a process that leads to the transformation of one set of chemical substances to another. Chemical reactions can be either spontaneous, requiring no input of energy, or non-spontaneous, typically following the input of some type of energy, such as heat, light or electricity...
.
A sand bath is most commonly used in conjunction with a hot plate
Hot plate
A hot plate is a portable self-contained tabletop small appliance that features one, two or more gas burners or electric heating elements. A hot plate can be used as a stand alone appliance, but is often used as a substitute for one of the burners from an oven range or the cook top of a stove...
or heating mantle
Heating mantle
Heating mantle or isomantle is a term for certain pieces of laboratory equipment used to apply heat to containers, as an alternative to other forms of heated bath...
. A beaker
Beaker (glassware)
A beaker is a simple container for stirring, mixing and heating liquids commonly used in many laboratories. Beakers are generally cylindrical in shape, with a flat bottom. Most also have a small spout to aid pouring as shown in the picture...
is filled with sand or metal pellets (called shot
Lead shot
Lead shot is a collective term for small balls of lead. These were the original projectiles for muskets and early rifles, but today lead shot is fired primarily from shotguns. It is also used for a variety of other purposes...
) and is placed on the plate or mantle. The reaction vessel is then partially covered by sand or pellets. The sand or shot then conducts the heat from the plate to all sides of the reaction vessel.
This technique allows a reaction vessel to be heated throughout with minimal stirring, as opposed to heating the bottom of the vessel and waiting for convection
Convection
Convection is the movement of molecules within fluids and rheids. It cannot take place in solids, since neither bulk current flows nor significant diffusion can take place in solids....
to heat the remainder, cutting down on both the duration of the reaction and the possibility of side reactions that may occur at higher temperatures.
A variation on this theme is the water bath
Water bath
A water bath can refer to:* A Bain-marie* A heated bath* A Laboratory water bath...
in which the sand is replaced with water. It can be used to keep a reaction vessel at the temperature of boiling water until all water is evaporated (see Standard enthalpy change of vaporization
Standard enthalpy change of vaporization
The enthalpy of vaporization, , also known as the heat of vaporization or heat of evaporation, is the energy required to transform a given quantity of a substance into a gas at a given pressure .It is often measured at the normal boiling point of a substance; although tabulated values are usually...
).
Sand baths are one of the oldest known pieces of laboratory equipment, having been used by the alchemists
Alchemy
Alchemy is an influential philosophical tradition whose early practitioners’ claims to profound powers were known from antiquity. The defining objectives of alchemy are varied; these include the creation of the fabled philosopher's stone possessing powers including the capability of turning base...
. In Arabic alchemy, a sand bath was known as a qadr. In Latin
Latin
Latin is an Italic language originally spoken in Latium and Ancient Rome. It, along with most European languages, is a descendant of the ancient Proto-Indo-European language. Although it is considered a dead language, a number of scholars and members of the Christian clergy speak it fluently, and...
alchemy, a sand bath was called balneum siccum, balneum cineritium, or balneum arenosum.